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Turn up your PCIE to max +0.35v ALWAYS this is what the bios does anyway when you set the voltage settings to normal. I hear vdroop is less when this is max. make sure you select Turbo at the top
You must set your RAM's timings manually, choose the x2.66D 400Mhz strap for your ram, most important setting to change is the tRD to 7 or higher, you can leave the other memory settings to AUTO
(G)MCH overvoltage I don't think is needed at these modest settings
Also give your memory extra volts to get it up to recommended high speed setting.
make sure no external devices are connected when attempting these new settings as a good o/c might fail for 'other' reasons
good luck
p.s give your cpu 1.525v just to make sure vdroop not stuffing you around
and try the CPU/PCIEx driving control at normal 800mv
p.s.s use the f5g bios as it has stated better quadcore and memory support, even though f5h should also be good , i haven't tried it.
p.s.s.s I can't get over 460fsb with mine, but my brothers q6600 goes at least 480FSB on a crappy Asus p5KC!!!!
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thank you Alcibiades